Reaction Calorimeter
RC HP 1000AE is a professional instrument designed to simulate chemical reactions at the liter scale, while measuring and controlling key process variables. As an automated reaction calorimeter for laboratory use, it can reproduce the real conditions of batch or semi-batch processes, and is widely applied in fine chemicals, pharmaceuticals, and third-party safety assessment for reaction process design, process optimization and scale-up, and process safety evaluation.
Test Parameters
Reaction process design, process optimization and scale-up, process safety evaluation
Application
Fine chemicals
Features
Specifications
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Features
Supports three calorimetric methods: heat-flow, power-compensation, and reflux calorimetry, allowing users to select according to application needs
Supports multiple operating modes, including isothermal, constant-temperature, and scanning modes
Compatible with optional glass atmospheric reactors, glass medium-pressure reactors, and metal high-pressure reactors
External reactor database enables one system to support interchangeable use of multiple reactors
High-power heating and cooling units provide fast temperature control response and high accuracy in heat-release measurement
Automatic reagent dosing with mass-based or volume-based control
Accurately measures and calculates process safety–related data, including reaction heat flow, reaction enthalpy, conversion rate, sample specific heat capacity, adiabatic temperature rise, and maximum temperature of the synthesis reaction (MTSR)
Software platform allows flexible experiment workflow configuration, real-time monitoring of key process data, and online modification of procedures and parameters
Real-time display of reactor temperature, jacket temperature, dosing amount, and other test status indicators
Configurable safety thresholds for key parameters and system status; one-click rapid cooling, abnormal-condition alarms, and automatic shutdown ensure safe operation during runaway events
Automatic generation and storage of charts and data, with export of experimental analysis reports
Specifications
Calorimetric Methods
Heat-flow calorimetry; power-compensation calorimetry (optional); reflux calorimetry (optional)
Temperature Control
| Reactor temperature range | −25 to 200 °C |
| Oil bath temperature range | −45 to 250 °C |
| Control modes | Isothermal, constant-temperature, scanning |
| Temperature resolution | 1.0 mK |
| Sample temperature control accuracy | ±0.1 K |
| Silicone oil circulation rate | 35–76 L/min |
Power Control
| Driver voltage range | 0–50 VDC |
| Max driver current | 3.0 A |
| Max heater power | 120 W |
Atmospheric Glass Reactor (Optional)
| Reactor volume | 1000 mL (other volumes customizable) |
| Operating pressure | Atmospheric |
| Reactor material | Glass |
Medium-Pressure Glass Reactor (Optional)
| Reactor volume | 1000 mL (other volumes customizable) |
| Operating pressure | 0.6 MPa or 1.2 MPa |
| Reactor body material | Glass |
| Reactor lid material | 316L stainless steel or Hastelloy |
High-Pressure Metal Reactor (Optional)
| Reactor volume | 1000 mL (other volumes customizable) |
| Operating pressure | 10 MPa |
| Reactor material | 316L stainless steel or Hastelloy |
Stirrer
| Max speed | 2000 rpm (optional 3000 rpm) |
| Max torque | 75 N·cm (optional 300 N·cm) |
| Impeller type | Anchor or paddle |
| Impeller material | PTFE, 316L stainless steel, or Hastelloy |
Dosing System
| Dosing channels | 1 liquid inlet, 1 solid charging port, 1 gas inlet; expandable up to 4 |
| Precision balance | Capacity 3100 g, readability 0.01 g |
| Medium-pressure pump | Electromagnetic diaphragm pump, max flow 2 L/h |
| High-pressure pump | Precision plunger pump, max flow 2.4 L/h |
Other Parameters
| Power supply | 3 × 400 V / 50 Hz (±10%) / 20 A |
| Power consumption | 7000 VA |
| Test area dimensions | 1200 mm × 600 mm × 1850 mm |
| Oil bath dimensions | 600 mm × 700 mm × 1300 mm |
| Oil bath weight | 210 kg |
| Total system weight | 300 kg |
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